بهینه‌سازی پارامترهای مؤثر بر سنتز باریم پراکسید به روش آماری تاگوچی

Norouzi, Mahdi; pourmortazavi, Seyed Mahdi; Kobadi Kerman, Saiedeh

Volume 19, Issue 4 (12-2024) مواد پرانرژی 2024, 19(4): 205-216 | Back to browse issues page

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Norouzi M, pourmortazavi S M, Kobadi Kerman S. بهینه‌سازی پارامترهای مؤثر بر سنتز باریم پراکسید به روش آماری تاگوچی. مواد پرانرژی 2024; 19 (4) :205-216
URL: http://isaem.ir/article-1-1525-en.html

بهینه‌سازی پارامترهای مؤثر بر سنتز باریم پراکسید به روش آماری تاگوچی

Mahdi Norouzi ^*

, Seyed Mahdi Pourmortazavi

, Saiedeh Kobadi Kerman

, mahdinorouzi58@yahoo.com

Abstract: (11 Views)

Barium peroxide has previously been employed as an oxidizer in the formulation of pyrotechnic compounds. The active oxygen content and the particle size of the oxidizer are two factors that influence the performance of pyrotechnic compounds. The active oxygen content and the particle size. In this study, the synthesis of barium peroxide was optimized with the objective of increasing the active oxygen content and reducing the particles size of the oxidiser. This was achieved through the application of the Taguchi statistical method. The synthesis of barium peroxide was evaluated at three levels for a range of parameters, including the concentration of barium hydroxide, the molar ratio of barium hydroxide to hydrogen peroxide, the rate of addition of hydrogen peroxide, the speed of stirring, the temperature, the mixing time and the drying conditions. The analysis of variance revealed that the optimal conditions for the synthesis of barium peroxide were hydrogen peroxide addition rate of 5 ml/min, mixing time of 0 min and rotary drying conditions. The resulting product had a minimum size of 6.03 microns. Similarly, under the optimal conditions of 1:1 molar ratio of barium hydroxide to hydrogen peroxide, 15-minute mixing time and vacuum drying conditions, barium peroxide with the highest oxygen content of 91.21% was prepared. The SEM), XRD and TGA/DSC analysis demonstrated the cluster morphology , barium peroxide with carbonate impurities and an onset of decomposition at temperatures above 500 °C, respectively.

Keywords: Barium Peroxide, Taguchi Method, particles size, active oxygen content

Full-Text [PDF 783 kb] (1 Downloads)

Type of Study: Research | Subject: سنتز، آناليز، کنترل کيفيت، فرمولاسيون و فرايندهاي توليد مواد پرانرژی (منفجره، پيروتکنيک و پيشرانه)
Published: 2025/09/3